Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dimethylformamide → 4-(3-Dimethylaminophenoxy)butyronitrile
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dimethylformamide | HCID 6228 | — |
| 반응물 | 3-(Dimethylamino)phenol | HCID 7421 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | 4-Bromobutyronitrile | HCID 21412 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 4-(3-Dimethylaminophenoxy)butyronitrile | HCID 21294517 | — |
반응 단계
A suspension of 3-dimethylaminophenol (5 g), potassium carbonate (10.05 g) and dimethylformamide (85 ml) was stirred at room temperature for 5 hours. 4-Bromobutyronitrile (7.3 ml) was added and the suspension stirred for 17 hours. The reaction mixture was poured into water and extracted with ethyl acetate. The extracts were washed with water, dried and the solvent removed to yield 4-(3-dimethylaminophenoxy)butyronitrile.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04767769 |
| 출처 데이터셋 | uspto-grants-1988_08 |
| ORD ID | ord-7c7eb924af47428b8286be45c1256f2f |
| 출처 메모 | uspto-grants-1988_08 |