Oxetane → HCID 131720936, 화합물

HRID 356221노트

반응식

[O:1]1[CH2:4][CH2:3][CH2:2]1.[C:5]1(=[O:11])[O:10][CH2:9][CH2:8][CH2:7][CH2:6]1.C([Al](CC)CC)C.O>>[C:5]1(=[O:11])[O:10][CH2:9][CH2:8][CH2:7][CH2:6]1.[O:1]1[CH2:4][CH2:3][CH2:2]1

참가 물질

반응물 3

HCID 10423Oxetane

HCID 10953Delta-Valerolactone

HCID 19429818Triethylalumane--water (1/1)

생성물 1

HCID 131720936HCID 131720936, 화합물

실험 절차

According to the ratio for charging as described in Table 2, oxetane and delta-valerolactone (referred to as VL in Table and Figure) were mixed, and polymerized in a bulk state at 60° C. for 24 hours using 0.2% by mol of a triethylaluminum-water (1/0.75) based complex as an initiator based on the total amount of the monomers.

후처리

additionwere mixed
custompolymerized in a bulk state at 60° C. for 24 hours

출처 및 근거

ORD 기록: ord-5eb6cc29799f4320bb7fc3e47e0a4563
출처 데이터셋: uspto-grants-1998_11
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05834567

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