4-tert-Butylcatechol → 1,2-Bis-(4-cyanophenoxy)-4-tert-butylbenzene

HRID 356236

반응식

HRID 356236 반응식
F[C:2]1[CH:9]=[CH:8][C:5]([C:6]#[N:7])=[CH:4][CH:3]=1.[C:10]([C:14]1[CH:15]=[C:16]([OH:21])[C:17](=[CH:19][CH:20]=1)[OH:18])([CH3:13])([CH3:12])[CH3:11]>>[C:6]([C:5]1[CH:8]=[CH:9][C:2]([O:18][C:17]2[CH:19]=[CH:20][C:14]([C:10]([CH3:13])([CH3:11])[CH3:12])=[CH:15][C:16]=2[O:21][C:2]2[CH:9]=[CH:8][C:5]([C:6]#[N:7])=[CH:4][CH:3]=2)=[CH:3][CH:4]=1)#[N:7]

참가 물질

3

반응물 2

HCID 73814-tert-ButylcatecholHCID 145174-Fluorobenzonitrile

생성물 1

HCID 218407281,2-Bis-(4-cyanophenoxy)-4-tert-butylbenzene수율 96.1%

실험 절차

The compound 4-fluorobenzonitrile was reacted with 4-tert-butylcatechol according to the procedure of Example 1. The product was recrystallized from methanol/water (3:1) to give a 96.1% yield of the title compound with the formula: ##STR12##

후처리

  1. customThe product was recrystallized from methanol/water (3:1)

출처 및 근거

ORD 기록
ord-7d545a34b1564b8aa47cfb8200e35964
출처 데이터셋
uspto-grants-1998_11
특허 번호
US05834620

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