Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl (4-nitrophenoxy)acetate → Methyl(4-aminophenoxy)acetate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl (4-nitrophenoxy)acetate | HCID 700522 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | Methyl(4-aminophenoxy)acetate | HCID 6422115 | 97.6% |
반응 단계
A procedure similar to that described in Example 6 was repeated, except that 30.8 g of methyl 4-nitro-phenoxyacetate (prepared as described in Preparation 36), 5.0 g of 10% w/w palladium-on-charcoal and 500 ml of methanol were used, to give 25.8 g of the title compound having Rf=0.79 (on silica gel thin layer chromatography using ethyl acetate as the developing solvent).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05834501 |
| 출처 데이터셋 | uspto-grants-1998_11 |
| ORD ID | ord-d75c053e7dda43a784c033be9ddf82c9 |
| 출처 메모 | uspto-grants-1998_11 |