Ethylamine → 4-bromo-N-ethylthiophene-3-carboxamide

HRID 356426

반응식

HRID 356426 반응식
[Br:1][C:2]1[C:3]([C:7]([OH:9])=O)=[CH:4][S:5][CH:6]=1.[CH2:10]([NH2:12])[CH3:11]>O>[CH2:10]([NH:12][C:7]([C:3]1[C:2]([Br:1])=[CH:6][S:5][CH:4]=1)=[O:9])[CH3:11]

참가 물질

4

반응물 2

HCID 6341EthylamineHCID 855464-Bromo-3-thenoic acid

생성물 1

HCID 186301214-bromo-N-ethylthiophene-3-carboxamide수율 64.5%

시약·촉매·용매 1

HCID 962Water용매

실험 절차

N-Ethyl-4-bromo-3-thiophenecarboxamide was prepared from 4-bromo-3-thiophenecarboxylic acid (7 g, 34 mmol) and 70% ethylamine in water according to steps a and b of Example 248 in 64.5% yield.

출처 및 근거

ORD 기록
ord-8bf33e9d685e4c08b67dc2d3e996617e
출처 데이터셋
uspto-grants-1998_11
특허 번호
US05834447

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