Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Imidazole → 4-(4-tert-Butyldimethylsilyloxy-phenyl)-2-butanone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Imidazole | HCID 795 | — |
| 반응물 | 4-(4'-Hydroxyphenyl)-2-butanone | HCID 21648 | — |
| 반응물 | tert-Butyldimethylsilyl chloride | HCID 28928 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | 4-(4-tert-Butyldimethylsilyloxy-phenyl)-2-butanone | HCID 18798666 | — |
반응 단계
The title compound was prepared as described in General Method 5 using 10 g (60.9 mmol) of 4-(4-hydroxyphenyl)-2-butanone, 10.1 g (67 mmol) of tert-butyldimethyl silyl chloride, 4.56 g (67 mmol) of imidazole and 150 mL of DMF. The crude product was carried on "as is" to the next step (see Example KK).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05834506 |
| 출처 데이터셋 | uspto-grants-1998_11 |
| ORD ID | ord-ffc34ceb05ed44a58e42ad7c9732bf74 |
| 출처 메모 | uspto-grants-1998_11 |