참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Formic Acid | HCID 284 | — |
| 반응물 | Water | HCID 962 | — |
| 반응물 | Dehydroepiandrosterone | HCID 5881 | — |
| 생성물 | 3beta-Formyloxy-androstene-17-one | HCID 131720941 | — |
반응 단계
Following the procedure described by Ringold (H. J. Ringold, et al., J. Am. Chem. Soc. 78, 816, 1956), dehydroepiandrosterone (2.88 g, 10 mmol) dissolved in 85% formic acid (100 mL) is heated at 60° C. for 1 h. After cooling, the mixture is poured into iced water and after 16 h, crystals are filtered and dried in vacuo.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05837700 |
|---|
| 출처 데이터셋 | uspto-grants-1998_11 |
|---|
| ORD ID | ord-c23a8e0841a64406bce4926a92eaf7b2 |
|---|
| 출처 메모 | uspto-grants-1998_11 |
|---|
