5,11-Dihydro-11-ethyl-5-methyl-2-trifluoromethanesulfonyloxy-6H-dipyrido[3,2-b:2',3'-e][1,4]diazepin-6-one → HCID 178462463, 화합물

HRID 356600노트

반응식

HRID 356600 반응식
[CH2:1]([N:3]1[C:9]2[N:10]=[CH:11][CH:12]=[CH:13][C:8]=2[C:7](=[O:14])[N:6]([CH3:15])[C:5]2[CH:16]=[CH:17][C:18](OS(C(F)(F)F)(=O)=O)=[N:19][C:4]1=2)[CH3:2].[CH3:28][C:29]1[C:33]([Sn](CCCC)(CCCC)CCCC)=[CH:32][NH:31][N:30]=1>>[CH2:1]([N:3]1[C:9]2[N:10]=[CH:11][CH:12]=[CH:13][C:8]=2[C:7](=[O:14])[N:6]([CH3:15])[C:5]2[CH:16]=[CH:17][C:18]([C:33]3[C:29]([CH3:28])=[N:30][NH:31][CH:32]=3)=[N:19][C:4]1=2)[CH3:2]

참가 물질

3

반응물 2

HCID 107160835,11-Dihydro-11-ethyl-5-methyl-2-trifluoromethanesulfonyloxy-6H-dipyrido[3,2-b:2',3'-e][1,4]diazepin-6-oneHCID 1784482253-Methyl-4-(tributylstannyl)pyrazole

생성물 1

HCID 178462463HCID 178462463, 화합물

실험 절차

The title compound (mp 113°-115° C.) was prepared from 5,11-dihydro-11-ethyl-5-methyl-2-trifluoromethanesulfonyloxy-6H-dipyrido[3,2-b:2',3'-e][1,4]diazepin-6-one and 3-methyl-4-(tributylstannyl)pyrazole in a manner analogous to that described in Example 1.

출처 및 근거

ORD 기록
ord-9b48e23aca544f51aec4429709c28d9a
출처 데이터셋
uspto-grants-1998_11
특허 번호
US05837704

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