Acrolein → HCID 13088566, 화합물

HRID 358017노트

반응식

HRID 358017 반응식
[C:1]([CH:5]=[CH:6][CH:7]=[CH2:8])([CH3:4])([CH3:3])[CH3:2].[CH:9]([CH:11]=[CH2:12])=[O:10].C(C1CCC(C=O)CC=1)(C)(C)C>>[C:1]([C:5]1[CH2:12][CH:11]([CH:9]=[O:10])[CH2:8][CH2:7][CH:6]=1)([CH3:4])([CH3:3])[CH3:2]

참가 물질

4

반응물 3

HCID 7847AcroleinHCID 1420695,5-Dimethyl-1,3-hexadieneHCID 13088567HCID 13088567, 화합물

생성물 1

HCID 13088566HCID 13088566, 화합물수율 30%

실험 절차

Molar amounts of tert.-butylbutadiene and acrolein are refluxed for 6-8 hours. A mixture of about 70% of 4-tert.-butyl-cyclohex-3-ene-1-carboxaldehyde and about 30% of 3-tert.-butyl-cyclohex-3-ene-1-carboxaldehyde is obtained in a yield of about 80%. Boiling point: 112° C./28 mbar.

출처 및 근거

ORD 기록
ord-9ca5366014a948e9a3738c128a37ac97
출처 데이터셋
uspto-grants-1984_08
특허 번호
US04464370

반응 노트

불러오는 중…