Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
tert-Butyl isocyanate → 1-Phenyl-3-t-butyl hydantoin
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | tert-Butyl isocyanate | HCID 62412 | — |
| 반응물 | N-Phenylglycine | HCID 66025 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | 1-Phenyl-3-t-butyl hydantoin | HCID 12263354 | 60% |
반응 단계
A mixture of N-phenyl glycine (0.1 mole), t-butyl isocyanate (0.12 mole) and toluene (30 ml) was refluxed for 5 hours and then cooled. The product was collected by filtration and crystallized from ethanol to produce 0.06 mole of the aforedescribed product having a melting point of 116° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04464387 |
| 출처 데이터셋 | uspto-grants-1984_08 |
| ORD ID | ord-0dbebeb7dd46429c87e48675660834df |
| 출처 메모 | uspto-grants-1984_08 |