Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Butyl isocyanate → 1-Phenyl-3-n-butyl hydantoin
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Butyl isocyanate | HCID 8110 | — |
| 반응물 | N-Phenylglycine | HCID 66025 | — |
| 생성물 | 1-Phenyl-3-n-butyl hydantoin | HCID 12459333 | 43.3% |
반응 단계
N-phenyl glycine (0.15 mole) was added with stirring over a 15 minute period to n-butyl isocyanate (0.15 mole). After the addition was complete the reaction mixture was refluxed for about 6 hours and then allowed to stand at room temperature until it solidified. The solidified mass was crystallized from ethanol and produced 0.065 moles of the above-described product having a melting point of 74° l C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04464387 |
| 출처 데이터셋 | uspto-grants-1984_08 |
| ORD ID | ord-8b448feab8ad457aab5c39656a815484 |
| 출처 메모 | uspto-grants-1984_08 |