Cyclohexyl isocyanate → 2,4-Imidazolidinedione, 3-cyclohexyl-1-phenyl-
반응식
[C:1]1([NH:7][CH2:8][C:9]([OH:11])=O)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH:12]1([N:18]=[C:19]=[O:20])[CH2:17][CH2:16][CH2:15][CH2:14][CH2:13]1>C1(C)C=CC=CC=1>[C:1]1([N:7]2[CH2:8][C:9](=[O:11])[N:18]([CH:12]3[CH2:17][CH2:16][CH2:15][CH2:14][CH2:13]3)[C:19]2=[O:20])[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1참가 물질
4
실험 절차
A mixture of N-phenyl glycine (0.1 mole), cyclohexyl isocyanate (0.12 mole) and toluene (30 ml) was refluxed for about 6 hours and then cooled. The crude product was recrystallized from ethanol to produce a 60% yield of the above-identified product having a melting point of approximately 196° C.
후처리
- temperaturewas refluxed for about 6 hours
- temperaturecooled
- customThe crude product was recrystallized from ethanol
출처 및 근거
- ORD 기록
- ord-66fce0b1974d45189e2f42748679d0bb
- 출처 데이터셋
- uspto-grants-1984_08
- 특허 번호
- US04464387
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