Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Undecanol → Undecyl propylcarbamate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Undecanol | HCID 8184 | — |
| 반응물 | Propyl isocyanate | HCID 61033 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | Undecyl propylcarbamate | HCID 20450444 | 89% |
반응 단계
For example, 8.6 g (50 mmol) of 1-undecanol, 5 ml (1.07 eq.) n-propyl isocyanate and 50 ml diethyl ether were heated in a stainless steel bomb at 65° for 72 hours. Solvent and excess isocyanate were removed on a rotary evaporator and the residue was crystallized from hexane to give 11.5 g (89%) of 1-undecyl propylcarbamate, mp 45°-45.5°.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04464390 |
| 출처 데이터셋 | uspto-grants-1984_08 |
| ORD ID | ord-7680ec264add46dfacb03dcd0912bcbd |
| 출처 메모 | uspto-grants-1984_08 |