Isopropanol → Isopropyl Trichloroacrylate
반응식
[CH:1]([OH:4])([CH3:3])[CH3:2].[Cl:5][C:6](=[C:10]([Cl:12])[Cl:11])[C:7](Cl)=[O:8]>C(Cl)Cl>[Cl:11][C:10]([Cl:12])=[C:6]([Cl:5])[C:7]([O:4][CH:1]([CH3:3])[CH3:2])=[O:8]참가 물질
4
실험 절차
A solution of 6.5 gms (0.108 moles) isopropyl alcohol, 20 gms (0.013 moles) trichloro acryloyl chloride and 100 ml methylene chloride was stirred for 72 hours. The solvent was stripped and the product was used in subsequent reactions without further purification.
후처리
- customthe product was used in subsequent reactions without further purification
출처 및 근거
- ORD 기록
- ord-4cc9112742054be59544a64647003c56
- 출처 데이터셋
- uspto-grants-1984_08
- 특허 번호
- US04465690
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