Methyl isothiocyanate → HCID 178486097, 화합물
반응식
[NH2:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[N:9]=[CH:10][NH:11][CH:12]=2)=[CH:4][CH:3]=1.[CH3:13][N:14]=[C:15]=[S:16]>C(O)C>[CH3:13][NH:14][C:15]([NH:1][C:2]1[CH:3]=[CH:4][C:5]([C:8]2[N:9]=[CH:10][NH:11][CH:12]=2)=[CH:6][CH:7]=1)=[S:16]참가 물질
4
실험 절차
A solution of 2.3 gm of 4-(4-aminophenyl)-1-H-imidazole and 1.15 gm of methyl isothiocyanate in 30 ml of ethanol was refluxed for thirty minutes and evaporated to dryness. The oily base so obtained was purified by conversion into the corresponding hydrochloride salt by bubbling gaseous hydrochloric acid in isopropanol. The desired thiourea was obtained as a white solid.
후처리
- customevaporated to dryness
- customThe oily base so obtained
- customwas purified by conversion into the corresponding hydrochloride salt
- customby bubbling gaseous hydrochloric acid in isopropanol
출처 및 근거
- ORD 기록
- ord-3b6a72acc242468fa129b70ab27e32a6
- 출처 데이터셋
- uspto-grants-1984_08
- 특허 번호
- US04465841
반응 노트
불러오는 중…