참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 3-Aminobenzoic Acid | HCID 7419 | — |
| 반응물 | 3-Ethoxy-2-propenoyl chloride | HCID 3014429 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | 3-[(3-Ethoxyacryloyl)amino]benzoic acid | HCID 54535487 | — |
반응 단계
100 Grams of m-aminobenzoic acid was suspended in 1 liter of diethyl ether, and at a room temperature with stirring 44.6 g of β-ethoxyacrylic chloride was added dropwise. Then the reaction mixture was heated at 40° C. for 5 hours. After the reaction was completed, the precipitated matter was collected by filtration and washed with water three times, and dried, and recrystallized from methanol to obtain 60 g of m-carboxy-N-(β-ethoxyacryloyl)aniline. Colorless cotton-like crystals. Melting point: 200.5°-202° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04468402 |
|---|
| 출처 데이터셋 | uspto-grants-1984_08 |
|---|
| ORD ID | ord-82ac0c8bc46149e89cfcb0ab00532117 |
|---|
| 출처 메모 | uspto-grants-1984_08 |
|---|
