반응식
[NH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][C:9]([OH:11])=[O:10].[Cl:12][C:13]1[S:14][C:15]([Cl:22])=[CH:16][C:17]=1[S:18](Cl)(=[O:20])=[O:19]>>[Cl:12][C:13]1[S:14][C:15]([Cl:22])=[CH:16][C:17]=1[S:18]([NH:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][C:9]([OH:11])=[O:10])(=[O:20])=[O:19]참가 물질
3
실험 절차
8-Aminocaprylic acid (1.0 g, 0.006 mole) was treated with 2,5-dichloro-3-thiophene sulphonyl chloride (1.58 g, 0.006 mole) according to the method described in Example 4 to give the title compound after recrystallisation from isopropanol/water (1.1 g, m.p. 92°-93° C.).
출처 및 근거
- ORD 기록
- ord-45be2263488a46599ac7cf730344e2d1
- 출처 데이터셋
- uspto-grants-1991_03
- 특허 번호
- US04997847
연결된 노트
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