Ammonia → Benzenesulfinamide

HRID 358746

반응식

HRID 358746 반응식
[C:1]1([S:7](Cl)=[O:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[NH3:10]>CCOCC>[C:1]1([S:7]([NH2:10])=[O:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

참가 물질

4

반응물 2

HCID 222AmmoniaHCID 4190003Benzenesulfinyl chloride

생성물 1

HCID 11286519Benzenesulfinamide수율 17%

시약·촉매·용매 1

HCID 3283Diethyl Ether용매

실험 절차

Benzenesulphinamide was prepared by reacting benzenesulphinyl chloride with ammonia in ether initially at -78° C. and finally at ambient temperature and was isolated in 17% yield as a solid, m.p. 112°-115° C.

후처리

  1. custominitially at -78° C.
  2. customfinally at ambient temperature and was isolated in 17% yield as a solid, m.p. 112°-115° C.

출처 및 근거

ORD 기록
ord-61f89b91a1154459a9933bf9d6056d4e
출처 데이터셋
uspto-grants-1991_03
특허 번호
US04997844

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