1,5-Dibromopentane → HCID 19101842, 화합물

HRID 358917

반응식

[C:1]1([CH2:11][OH:12])[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][CH:2]=1.[Br:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18]Br>>[Br:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][O:12][CH2:11][C:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][CH:2]=1

참가 물질

반응물 2

HCID 81001,5-Dibromopentane

HCID 209081-Naphthalenemethanol

생성물 1

HCID 19101842HCID 19101842, 화합물

실험 절차

1-Naphthalenemethanol (6.00 g) and 1,5-dibromopentane (11.5 ml) were treated according to the method of Intermediate 1. FCC eluting with ether-cyclohexane (1:49→2:48) gave the title compound as a colourless oil (8.41 g), t.l.c. (Cyclohexane-ether 19:1) Rf 0.22;

후처리

washFCC eluting with ether-cyclohexane (1:49→2:48)

출처 및 근거

ORD 기록: ord-4611bcd69430414db39cf9c80118e4c3
출처 데이터셋: uspto-grants-1991_03
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04997986

연결된 노트

불러오는 중…