Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Tatb → 1,3,5-Trichloro-2,4,6-trinitrobenzene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Tatb | HCID 18286 | — |
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | 1,3-Dichloro-5-methoxy-2,4,6-trinitrobenzene | HCID 14794057 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | 1,3,5-Trichloro-2,4,6-trinitrobenzene | HCID 17518 | — |
반응 단계
Preparation of 1,3,5-triamino-2,4,6-trinitrobenzene (TATB) from 3,5-dichloroanisole. Nitration of 3,5-dichloroanisole under relatively mild conditions gave 3,5-dichloro-2,4,6-trinitroanisole in high yield and purity. Ammonolysis of this latter compound gave the desired TATB. Another route to TATB was through the treatment of the 3,5-dichloro-2,4,6-trinitroanisole with thionyl chloride and dimethylformamide to yield 1,3,5-trichloro-2,4,6-trinitrobenzene. Ammonolysis of this product produced TATB.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04997987 |
| 출처 데이터셋 | uspto-grants-1991_03 |
| ORD ID | ord-6e34c9a50fef40368a5c0a0a0abf8e7d |
| 출처 메모 | uspto-grants-1991_03 |