참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 4-Chlorophenol | HCID 4684 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | 1-Bromo-4-nitrobenzene | HCID 11466 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 1-Chloro-4-(4-nitrophenoxy)benzene | HCID 15786 | 95% |
반응 단계
p-Chlorophenol (7 g), p-nitrobromobenzene (11.0 g) and potassium carbonate (9.02 g) in dimethylsufoxide (35 ml) were heated with stirring at 120° C. for 24 hours and cooled, and the mixture was poured into water. The resulting precipitate was collected by filtration and washed with water. The resultant was heated in a mixed solvent of methanol/water [4:1,(v/v)], and allowed to cool. The resulting product was collected by filtration to give 4-(4-chlorophenoxy)nitrobenzene (12.92 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04999378 |
|---|
| 출처 데이터셋 | uspto-grants-1991_03 |
|---|
| ORD ID | ord-abd26f5b9827450e90a5f585c85651fe |
|---|
| 출처 메모 | uspto-grants-1991_03 |
|---|
