Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Phenanthro[1,2-b]furan-2-methanol → Phenanthro[1,2-b]thiophene-2-methanol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Phenanthro[1,2-b]furan-2-methanol | HCID 14770239 | — |
| 반응물 | Ethyl phenanthro[1,2-b]thiophene-2-carboxylate | HCID 14770247 | — |
| 용매 | Methylenechloride Hexane | HCID 21226440 | — |
| 생성물 | Phenanthro[1,2-b]thiophene-2-methanol | HCID 14770248 | 98% |
반응 단계
Using the procedure outlined in 14A, ethyl phenanthro[1,2-b]thiophene-2-carboxylate (H. G. Pars Pharmaceutical Laboratories, Inc.) gave a 98.0% yield of phenanthro[1,2-b]thiophene-2-methanol, mp 169°-170.5° (C,H,S), (CH2Cl2 /hexane).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04999369 |
| 출처 데이터셋 | uspto-grants-1991_03 |
| ORD ID | ord-4be1c16d46ce430098ad61634db58075 |
| 출처 메모 | uspto-grants-1991_03 |