Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Dodecylaniline → HCID 20064821, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Dodecylaniline | HCID 7701 | — |
| 반응물 | AG-G-77560 | HCID 2778031 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | HCID 20064821 | HCID 20064821 | — |
반응 단계
A 2.3-g portion (0.005 mole) of 2,4,6-triphenylpyrylium triflate is placed in a 500-ml round-bottom flask. To this, 200 ml of ethanol is added and then 1.3 g (0.005 mole) of p-dodecylaniline is added. The mixture is refluxed for about 20 hours. The ethanol is removed by evaporation to give a yellow waxy substance. This material is washed with ether which causes some yellow crystals to precipitate.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05000873 |
| 출처 데이터셋 | uspto-grants-1991_03 |
| ORD ID | ord-7f3fcc1c6d9047fca8c49414a0df1a8c |
| 출처 메모 | uspto-grants-1991_03 |