4-Dodecylaniline → HCID 20064821, 화합물

HRID 359306

반응식

HRID 359306 반응식
[O-:1][S:2]([C:5]([F:8])([F:7])[F:6])(=[O:4])=[O:3].[C:9]1([C:15]2[CH:20]=[C:19](C3C=CC=CC=3)C=C(C3C=CC=CC=3)[O+]=2)[CH:14]=C[CH:12]=[CH:11][CH:10]=1.[CH2:33]([C:45]1[CH:51]=[CH:50][C:48]([NH2:49])=[CH:47][CH:46]=1)[CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH2:39][CH2:40][CH2:41][CH2:42][CH2:43][CH3:44]>C(O)C>[O-:4][S:2]([C:5]([F:8])([F:7])[F:6])(=[O:3])=[O:1].[CH2:33]([C:45]1[CH:46]=[CH:47][C:48]([N+:49]2[C:20]([CH3:19])=[CH:15][C:9]([CH3:14])=[CH:10][C:11]=2[CH3:12])=[CH:50][CH:51]=1)[CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH2:39][CH2:40][CH2:41][CH2:42][CH2:43][CH3:44]

참가 물질

4

반응물 2

HCID 77014-DodecylanilineHCID 2778031AG-G-77560

생성물 1

HCID 20064821HCID 20064821, 화합물

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

A 2.3-g portion (0.005 mole) of 2,4,6-triphenylpyrylium triflate is placed in a 500-ml round-bottom flask. To this, 200 ml of ethanol is added and then 1.3 g (0.005 mole) of p-dodecylaniline is added. The mixture is refluxed for about 20 hours. The ethanol is removed by evaporation to give a yellow waxy substance. This material is washed with ether which causes some yellow crystals to precipitate.

후처리

  1. temperatureThe mixture is refluxed for about 20 hours
  2. customThe ethanol is removed by evaporation
  3. customto give a yellow waxy substance
  4. washThis material is washed with ether which
  5. customto precipitate

출처 및 근거

ORD 기록
ord-7f3fcc1c6d9047fca8c49414a0df1a8c
출처 데이터셋
uspto-grants-1991_03
특허 번호
US05000873

연결된 노트

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