Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzoyl isothiocyanate → 2-[[(Benzoylamino)thioxomethyl)amino]-5-methylbenzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzoyl isothiocyanate | HCID 68284 | — |
| 반응물 | 2-Amino-5-methylbenzamide | HCID 10329436 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | 2-[[(Benzoylamino)thioxomethyl)amino]-5-methylbenzamide | HCID 15135526 | 92.7% |
반응 단계
To a stirred mixture of 4.5 g of 2-amino-5-methylbenzamide and 200 ml of ether was added dropwise, a solution of 4.9 g benzoyl isothiocyanate in 100 ml of ether over 20 minutes. After stirring overnight, the solid was collected, giving 8.7 g of the desired product as white crystals, mp 198°-201° C. (dec.).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05001157 |
| 출처 데이터셋 | uspto-grants-1991_03 |
| ORD ID | ord-bf226b19b1494fbcb2fcb721767d0361 |
| 출처 메모 | uspto-grants-1991_03 |