Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Methylbenzoyl isothiocyanate → HCID 15135527, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Methylbenzoyl isothiocyanate | HCID 140139 | — |
| 반응물 | 2-Amino-5-methylbenzamide | HCID 10329436 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | HCID 15135527 | HCID 15135527 | 91.7% |
반응 단계
To a stirred mixture of 3 g of 2-amino-5-methylbenzamide and 200 ml of ether was added dropwise, a solution of 3.7 g of 4-methylbenzoyl isothiocyanate in 100 ml of ether over 3 minutes. After 24 hours, the solid was collected, giving 6 g of the desired product as off-white crystals, mp 208°-209° C. (dec.).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05001157 |
| 출처 데이터셋 | uspto-grants-1991_03 |
| ORD ID | ord-4069010e62c24b25b7663212dfb2f6b7 |
| 출처 메모 | uspto-grants-1991_03 |