Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Allylamine → 2,2'-Azobis[n-(2-propenyl)-2-methylpropionamide]
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Allylamine | HCID 7853 | — |
| 반응물 | 1,1'-Dimethyl 2,2'-(1,2-diazenediyl)bis(2-methylpropanoate) | HCID 75763 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 2,2'-Azobis[n-(2-propenyl)-2-methylpropionamide] | HCID 15724735 | — |
반응 단계
Dimethyl 2,2'-azobis(2-methylpropionate) in an amount of 41.9 g, 48 ml of methanol, and 43 g of a 28% CH3ONa methanol solution were mixed and stirred for dissolution, followed by dropwise addition of 25 g of allylamine to react at 19° to 21° C. for 20 hours.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05001228 |
| 출처 데이터셋 | uspto-grants-1991_03 |
| ORD ID | ord-cbc849f2079f4b2e89bfcd0e603da8a8 |
| 출처 메모 | uspto-grants-1991_03 |