Nitrogen → 1,4-Dichlorobenzene

HRID 359611

반응식

HRID 359611 반응식
N#N.[Cl:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1.[Cl:10][C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][C:12]=1[Cl:17]>>[Cl:3][C:4]1[CH:9]=[CH:8][CH:7]=[C:6]([Cl:10])[CH:5]=1.[CH:16]1[C:15]([Cl:3])=[CH:14][CH:13]=[C:12]([Cl:17])[CH:11]=1.[Cl:10][C:11]1[C:12]([Cl:17])=[C:13]([Cl:3])[CH:14]=[CH:15][CH:16]=1

참가 물질

6

반응물 3

HCID 947NitrogenHCID 72391,2-DichlorobenzeneHCID 7964Chlorobenzene

생성물 3

HCID 46851,4-DichlorobenzeneHCID 68951,2,3-TrichlorobenzeneHCID 109431,3-Dichlorobenzene

실험 절차

In general, the flow rate (30 mls/min) of the carrier gas (N2) and the column temperature (130° C. isothermal for 30 mins) were optimized to provide baseline resolution for the simultaneous analyses of chlorobenzene, m-dichlorobenzene, p-dichlorobenzene, o-dichlorobenzene and trichlorobenzene.

후처리

  1. customthe column temperature (130° C. isothermal for 30 mins)

출처 및 근거

ORD 기록
ord-1c6f0a9cb6e8456a9c63290e204eafc7
출처 데이터셋
uspto-grants-1991_03
특허 번호
US05001290

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