Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetyl chloride → HCID 137226513, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetyl chloride | HCID 6367 | — |
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | Ethanediimidoyl dichloride, dihydroxy- | HCID 135527345 | — |
| 용매 | 1,1-Dichloroethane | HCID 6365 | — |
| 생성물 | HCID 137226513 | HCID 137226513 | 30% |
반응 단계
The mixture of 2.0 g (0.0127 mol) of dichloroglyoxime (Compound No.6), 20 ml of dichloroethane and 2.4 g (0.0306 mol) of acetyl chloride was stirred in an ice bath. To the mixture, triethylamine (3.1 g, 0.0307 mol) was added dropwise, followed by stirring for 30 minutes. The reaction mixture was washed twice with 15 ml of water. The dichloroethane solution was concentrated under reduced pressure, to obtain white crystals of dichloroglyoxime diacetate (Compound No.2, yield: 30%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05411990 |
| 출처 데이터셋 | uspto-grants-1995_05 |
| ORD ID | ord-8cf7e900532942bd97b5cb69fa438ac1 |
| 출처 메모 | uspto-grants-1995_05 |