Ethanethioic acid, S-(2-chloro-2-oxoethyl) ester → HCID 178460282, 화합물

HRID 35970

반응식

HRID 35970 반응식
C(S[CH2:5][C:6]([NH:8][C@H:9]1[CH2:14][CH2:13][C@H:12]([O:15][N+:16]([O-:18])=[O:17])[CH2:11][CH2:10]1)=[O:7])(=O)C.O([C@H:23]1CC[C@H](N)CC1)[N+]([O-])=O.C(SCC(Cl)=O)(=O)C>>[C:6]([NH:8][C@H:9]1[CH2:14][CH2:13][C@H:12]([O:15][N+:16]([O-:18])=[O:17])[CH2:11][CH2:10]1)(=[O:7])[CH2:5][CH3:23]

참가 물질

4

반응물 3

HCID 82724Ethanethioic acid, S-(2-chloro-2-oxoethyl) esterHCID 178477142HCID 178477142, 화합물HCID 178511725HCID 178511725, 화합물

생성물 1

HCID 178460282HCID 178460282, 화합물수율 67%

실험 절차

2-acetylmercapto-N-(trans-4-nitroxycyclohexyl)acetic acid amide from trans-4-nitroxycyclohexylamine and 2-acetylmercaptoacetic acid chloride melting point: 127°-129° C. (ether), yield: 67% of theory.

출처 및 근거

ORD 기록
ord-086d97b933f84449a5902622d6ad17f2
출처 데이터셋
uspto-grants-1995_05
특허 번호
US05411989

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