Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl 4-bromobenzoate → 2'-[2-(1-methyl-1-phenylethyl)-2H-tetrazol-5-yl]biphenyl-4-carboxylic acid methyl ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl 4-bromobenzoate | HCID 12081 | — |
| 반응물 | 5-phenyl-2-(2-phenylpropan-2-yl)-2H-tetrazole | HCID 1289594 | — |
| 촉매 | Nickel | HCID 935 | — |
| 생성물 | 2'-[2-(1-methyl-1-phenylethyl)-2H-tetrazol-5-yl]biphenyl-4-carboxylic acid methyl ester | HCID 11825483 | — |
반응 단계
reacting the ortho-transmetalated 2-(1-methyl-1-phenylethyl)-5-phenyl-2H-tetrazole with methyl 4-bromobenzoate in the presence of phosphinated nickel catalyst to give 2'-[2-(1-methyl-1-phenylethyl)-2H-tetrazol-5-yl]biphenyl-4-carboxylic acid methyl ester,
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05412102 |
| 출처 데이터셋 | uspto-grants-1995_05 |
| ORD ID | ord-a73cc2a80fb64f3eb36602803309cbc2 |
| 출처 메모 | uspto-grants-1995_05 |