Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Alumina → Methyl cyclohexanecarboxylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Alumina | HCID 9989226 | — |
| 반응물 | Dimethyl Cyclohexane-1,1-dicarboxylate | HCID 10965525 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | Methyl cyclohexanecarboxylate | HCID 20748 | 316% |
반응 단계
Per hour a solution of 4.5 g of dimethyl 1,1-cyclohexanedicarboxylate in 4.5 g of methanol was passed at 275° C. over 5 g of aluminum oxide. The exit mixture obtained over 6 hours (36.5 g) was distilled to yield 10.1 g of methyl cyclohexanecarboxylate (53%, based on diester used) and 7.7 g of the starting material.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05412120 |
| 출처 데이터셋 | uspto-grants-1995_05 |
| ORD ID | ord-2cbfd30ef447489789c90ee246ab483c |
| 출처 메모 | uspto-grants-1995_05 |