Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thionyl Chloride → 3-methoxy-4-nitro-benzoyl Chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | 3-Methoxy-4-nitrobenzoic acid | HCID 78764 | — |
| 용매 | 2,2,4-Trimethylpentane | HCID 10907 | — |
| 생성물 | 3-methoxy-4-nitro-benzoyl Chloride | HCID 11127655 | — |
반응 단계
A stirred suspension of 1.0 g of 3-methoxy-4-nitrobenzoic acid and 1.40 ml of thionyl chloride is heated to reflux for 2 hours. The mixture is cooled to room temperature, 2 ml of iso-octane added and the mixture evaporated in vacuo to a solid residue. The residue is washed with iso-octane (2×2 ml), dried in vacuo to give 1.08 g of cream colored solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05733905 |
| 출처 데이터셋 | uspto-grants-1998_03 |
| ORD ID | ord-bb6cde0faedc4e19ba217101110ea105 |
| 출처 메모 | uspto-grants-1998_03 |