참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Dimethylformamide | HCID 6228 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | N-Butylaniline | HCID 14310 | — |
| 반응물 | 2-Bromoheptane | HCID 16090 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | N-Butyl-N-(heptan-2-YL)aniline | HCID 18000381 | 60% |
반응 단계
A mixture of N-butylaniline (7.45 parts) anhydrous potassium carbonate (7.5 parts), 2-bromoheptane (13.5 parts) and DMF (25 parts) was stirred at 130° C. for 86 hours. The reaction mixture was poured into water, saturated with salt and extracted with ethyl acetate. The organic phase was washed with water, dried (MgSO4) and evaporated to leave N-butyl-N-(1-methylhexyl)aniline (11.8 parts, approximately 60% strength). This material had acetic anhydride (10 parts) added to it prior to further use.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05865857 |
|---|
| 출처 데이터셋 | uspto-grants-1999_02 |
|---|
| ORD ID | ord-b013d208f9804c31a1bf4f08faa23737 |
|---|
| 출처 메모 | uspto-grants-1999_02 |
|---|
