참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Dimethylformamide | HCID 6228 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | Benzenamine, N-propyl- | HCID 12153 | — |
| 반응물 | 2-Ethylhexyl bromide | HCID 86804 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | N-(2-ethylhexyl)-N-propylaniline | HCID 53707404 | 89% |
반응 단계
A mixture of N-propylaniline (24 parts), 2-ethylhexyl bromide (58 parts), anhydrous potassium carbonate (42 parts) and dry N,N-dimethylformamide (50 parts) was stirred at 125° C. for 16 hours. The cooled reaction mixture was poured into water (250 parts), the organic phase separated and washed with water (2×200 parts) and dried at 90° C. and 15 mmHg to yield N-(2-ethylhexyl)-N-propylaniline (49 parts, 89%). Acetic anhydride was added to this to make a total of 69.5 parts.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05865857 |
|---|
| 출처 데이터셋 | uspto-grants-1999_02 |
|---|
| ORD ID | ord-e8c4b4af7a854ceba4a19e440aee6972 |
|---|
| 출처 메모 | uspto-grants-1999_02 |
|---|
