참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Aniline | HCID 6115 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | 2-Ethylhexyl bromide | HCID 86804 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | N-(2-Ethylhexyl)aniline | HCID 61484 | 43% |
반응 단계
A mixture of aniline (18.6 parts), 2-ethylhexyl bromide (42.4 parts), anhydrous potassium carbonate (30.3 parts) and dry N,N-dimethylformamide (100 parts) was stirred at 75° C. for 24 hours. The cooled mixture was filtered, diluted with dichloromethane and washed with 2N-hydrochloric acid (100 parts). The organic phase was evaported to leave oil which was triturated with petroleum ether and water to give N-(2-ethylhexyl)aniline (18 parts, 43%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05865857 |
|---|
| 출처 데이터셋 | uspto-grants-1999_02 |
|---|
| ORD ID | ord-a1f10645be1845a384339f2e205461d5 |
|---|
| 출처 메모 | uspto-grants-1999_02 |
|---|
