O-Xylene → HCID 18788042, 화합물

HRID 361287

반응식

HRID 361287 반응식
[CH2:1]([N:5](CC(C)=C)[C:6]1[CH:11]=CC=C[CH:7]=1)[CH2:2][CH2:3][CH3:4].[C:16]1([CH3:23])[C:17](C)=[CH:18][CH:19]=[CH:20][CH:21]=1>[Cl-].[Zn+2].[Cl-]>[CH2:1]([N:5]1[C:17]2[C:16](=[CH:21][CH:20]=[CH:19][CH:18]=2)[CH2:23][C:6]1([CH3:11])[CH3:7])[CH2:2][CH2:3][CH3:4]

참가 물질

4

반응물 2

HCID 7237O-XyleneHCID 54010992N-butyl-N-(2-methylprop-2-eneyl)aniline

생성물 1

HCID 18788042HCID 18788042, 화합물

시약·촉매·용매 1

HCID 3007855Zincchloride촉매

실험 절차

A mixture of N-butyl-N-(2-methylprop-2-eneyl)aniline (9.6 parts), zinc chloride (6.12 parts) and xylene (20 parts) was heated under reflux with vigorous stirring for 4.75 hours. The cooled mixture was filtered and the organic phase evaporated to leave 1-butyl-2,2-dimethylindoline (5.3 parts).

후처리

  1. temperaturewas heated
  2. temperatureunder reflux
  3. filtrationThe cooled mixture was filtered
  4. customthe organic phase evaporated

출처 및 근거

ORD 기록
ord-c307e14b853947698fc2fcb3cdb64320
출처 데이터셋
uspto-grants-1999_02
특허 번호
US05865857

연결된 노트

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