Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N-heptylacetamide → 1-Heptanamine, N-ethyl-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N-heptylacetamide | HCID 347488 | — |
| 반응물 | Aluminium lithium hydride | HCID 21226445 | — |
| 반응물 | Sodium hydroxide--water (1/1/1) | HCID 23719242 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | 1-Heptanamine, N-ethyl- | HCID 48038 | — |
반응 단계
A mixture of a solution of 5.5 gms of the N-heptylacetamide in 150 ml of diethyl ether and 3.99 gms of lithium aluminum hydride are stirred at room temperature for 18 hours. The reaction mixture is then worked up with H2O/NaOH by the Fieser method, following which the organic layer is dried over MgSO4, filtered, and concentrated under vacuum to give N-heptyl-N-ethylamine.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05412137 |
| 출처 데이터셋 | uspto-grants-1995_05 |
| ORD ID | ord-f3528eb525984558858b648e2ac6c3f7 |
| 출처 메모 | uspto-grants-1995_05 |