참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Nitric Acid | HCID 944 | — |
| 반응물 | 2,6-Dichloro-4'-methoxy-2'-methyl-benzophenone | HCID 54505258 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 2,6-Dichloro-5'-nitro-4'-methoxy-2'-methyl-benzophenone | HCID 54492291 | — |
반응 단계
2,6-Dichloro-4'-methoxy-2'-methyl-benzophenone (0.75 g; 2.5 mmol) is added to nitric acid (10 ml; 65%). The mixture is stirred at 80° C. for 1hour. After addition of water the reaction product crystallises and is chromatographically purified (flash column filled with 30 g of silicagel, elution with toluene). White crystals (0.35 g; 41% y); mp. 156°-160° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05866722 |
|---|
| 출처 데이터셋 | uspto-grants-1999_02 |
|---|
| ORD ID | ord-7ffdccfbac954e48aa3458fa8a6fa77a |
|---|
| 출처 메모 | uspto-grants-1999_02 |
|---|
