Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thionyl Chloride → 4-[(2-methylbenzoyl)amino]benzoyl Chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | 4-[(2-methylbenzoyl)amino]benzoic Acid | HCID 11615814 | — |
| 생성물 | 4-[(2-methylbenzoyl)amino]benzoyl Chloride | HCID 10707441 | — |
반응 단계
A mixture of 10.3 g of 4-[(2-methylbenzoyl)amino]benzoic acid and 32 ml of thionyl chloride is refluxed for 1.5 hours. The solution is concentrated under vacuum. Toluene is added and the solvent removed under vacuum. Toluene is added and the mixture chilled and filtered to give a yellow solid, m.p. 135°-141° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05869483 |
| 출처 데이터셋 | uspto-grants-1999_02 |
| ORD ID | ord-8acafb79f0d54b23bd91fbcf82dadbee |
| 출처 메모 | uspto-grants-1999_02 |