Imidazole → Imidazole isocyanuric acid

반응식

[NH:1]1[CH:5]=[CH:4][N:3]=[CH:2]1.[NH:6]1[C:13](=[O:14])[NH:12][C:10](=[O:11])[NH:9][C:7]1=[O:8]>>[NH:1]1[CH:5]=[CH:4][N:3]=[CH:2]1.[NH:6]1[C:13](=[O:14])[NH:12][C:10](=[O:11])[NH:9][C:7]1=[O:8]

참가 물질

반응물 2

HCID 795Imidazole

HCID 7956Cyanuric acid

생성물 1

HCID 68522078Imidazole isocyanuric acid

실험 절차

Heretofore, in a process for obtaining an adduct of imidazole-isocyanuric acid, water, aqueous solution of acetic acid, or dimethylformamide is used as a solvent. An imidazole compound and isocyanuric acid are charged into the solvent as it is in a solid to react by addition, and then crystallized while cooling, thereby being obtained an adduct of imidazole-isocyanuric acid. (confer JP-A-53-116391).

후처리

customto react by addition
customcrystallized
temperaturewhile cooling

출처 및 근거

ORD 기록: ord-523eaac753074f7b8ebf4e8ee6e19117
출처 데이터셋: uspto-grants-1999_02
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05869664

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