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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 362828생성일: 2026년 10월 25일

Ethyl 3-(2-fluorophenyl)prop-2-enoate → Ethyl 3-(2-fluorophenyl)propanoate

https://huagongshe.com/reaction/362828

반응식

참여 물질

역할이름HCID투입량
반응물Ethyl 3-(2-fluorophenyl)prop-2-enoateHCID 590919—
반응물HCID 178418361HCID 178418361—
촉매Platinum oxide monohydrateHCID 86587499—
용매EthanolHCID 702—
생성물Ethyl 3-(2-fluorophenyl)propanoateHCID 1487901499%

반응 단계

A mixture of ethyl 2-fluorocinnamate (29.25 g, 0.176 mol) and platinum oxide hydrate (0.25, EM Scientific) in 95% ethanol (150 mL) was placed on a Parr hydrogenation apparatus and shaken under 2-4 atm at hydrogen pressure. After the appropriate amount of hydrogen was consumed, the catalyst was removed by filtration, and the filtrate was concentrated in vacuo to give 29.39 g (99%) of crude ethyl 3-(2-fluorophenyl)propionate. This material was used without further purification.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05872118
출처 데이터셋uspto-grants-1999_02
ORD IDord-804027412b4e4b3593bfa9c776543599
출처 메모uspto-grants-1999_02