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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 363038생성일: 2026년 10월 26일

Methyl 3-allyl-4-hydroxybenzoate → Methyl 4-hydroxy-3-propylbenzoate

https://huagongshe.com/reaction/363038

반응식

참여 물질

역할이름HCID투입량
반응물Methyl 3-allyl-4-hydroxybenzoateHCID 939882—
촉매PalladiumHCID 23938—
용매Ethyl AcetateHCID 8857—
생성물Methyl 4-hydroxy-3-propylbenzoateHCID 11805593—

반응 단계

To 22-3 (6.0 g, 33.2 mmol) in 50 mL of EtOAc was added 60 mg of 5% Pd on carbon and the whole was hydrogenated at atmospheric pressure for 24 h. Hydrogen was removed from the reaction mixture and the solution was filtered through Celite. Evaporation of the solvent afforded product 22-4 as a white solid.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05872138
출처 데이터셋uspto-grants-1999_02
ORD IDord-f01451e0f3f640d8932c8f76d798ecf0
출처 메모uspto-grants-1999_02