Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-(Benzyloxy)phenyl benzoate → p-Hydroxyphenyl benzoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-(Benzyloxy)phenyl benzoate | HCID 241255 | — |
| 반응물 | HCID 178418361 | HCID 178418361 | — |
| 촉매 | HCID 178418390 | HCID 178418390 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | p-Hydroxyphenyl benzoate | HCID 75549 | 94% |
반응 단계
A reaction vessel was charged with 38 g of 4-benzyloxyphenyl benzoate and 500 ml of ethanol, and the air in the vessel was replaced with nitrogen. Then, 1.0 g of 10% palladium carbon was added thereto, and the nitrogen in the vessel was replaced with hydrogen, followed by vigorous stirring at room temperature for 24 hours. The hydrogen in the vessel was replaced with nitrogen, after which the reaction mixture was filtered though celite, and the filtrate was concentrated, which afforded 24.5 g of 4-hydroxyphenyl benzoate (94% yield).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05872137 |
| 출처 데이터셋 | uspto-grants-1999_02 |
| ORD ID | ord-a929d519d72544c49f384c6363083c0c |
| 출처 메모 | uspto-grants-1999_02 |