Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethanol → ethyl N-n-octanoylanthranilate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethanol | HCID 702 | — |
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | 2-(Octanoylamino)benzoic acid | HCID 4157220 | — |
| 생성물 | ethyl N-n-octanoylanthranilate | HCID 4179835 | 89.2% |
반응 단계
Thionyl chloride was dropped to ethanol and the mixture was stirred for 2 hours. Then, N-n-octanoylanthranilic acid was added to the mixture and reaction was allowed to proceed for 3 days at the room temperature. After the reaction, the solvent was removed and ethyl N-n-octanoylanthranilate was obtained from the remaining reactant after the purification by column chromatography with the yield of 89.2 %.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05413794 |
| 출처 데이터셋 | uspto-grants-1995_05 |
| ORD ID | ord-6973f46854414d4d8229c43ebb702f0c |
| 출처 메모 | uspto-grants-1995_05 |