Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → 5-phenylpyridine-2-carboxylic Acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | 2-Methyl-5-phenylpyridine | HCID 76744 | — |
| 반응물 | Potassium Permanganate | HCID 516875 | — |
| 생성물 | 5-phenylpyridine-2-carboxylic Acid | HCID 2762870 | — |
반응 단계
A suspension of 3-phenyl-6-methyl pyridine (1.99 g, 11.78 mmol) and potassium permanganate (7.65, 48.6 mmol), in water (50 mL) was heated at reflux for 16 hours. The reaction was allowed to cool to ambient temperature and filtered through celite to remove the solids. Acetic acid (2 mL) was added to the colourless filtrate and the product was collected as a white solid by filtration.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05872136 |
| 출처 데이터셋 | uspto-grants-1999_02 |
| ORD ID | ord-343691b2d04c48aca1c08a10cca1ee35 |
| 출처 메모 | uspto-grants-1999_02 |