Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Tetrabutylammonium Hydroxide → Tetrabutylammonium
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Tetrabutylammonium Hydroxide | HCID 2723671 | — |
| 반응물 | 2-Amino-6-iodopurine | HCID 6101575 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | Tetrabutylammonium | HCID 16028 | — |
| 생성물 | 2-Amino-6-iodopurine | HCID 6101575 | — |
반응 단계
To a mixture of 6-iodo-2-aminopurine (1.21 g., 4.637 mmole) in methylene chloride (12 ml.) at room temperature, was added 1.5M tetra(n-butyl)ammonium hydroxide (2.7 ml., 4.05 mmole). The reaction mixture was stirred for 10 minutes, and the volatiles were removed in vacuo. Methylene chloride (12 ml.) was added to the white residue, and the resulting solution was dried (magnesium sulfate), filtered, and the filtrate was concentrated in vacuo to yield the tetra(n-butyl)ammonium salt of 6-iodo-2-aminopurine as a white residue.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05414000 |
| 출처 데이터셋 | uspto-grants-1995_05 |
| ORD ID | ord-b08e4d29c6fd4228ab53668cb15e5f1a |
| 출처 메모 | uspto-grants-1995_05 |