참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Toluene | HCID 1140 | — |
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | 4-Amino-3-chloro-5-methoxyiminomethylbenzoic acid | HCID 54099134 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | 4-Amino-3-chloro-5-methoxyiminomethylbenzoyl chloride | HCID 54454051 | — |
반응 단계
In a 5-liter three-necked round-bottomed flask was placed 180 g of the previously prepared 4-amino-3-chloro-5-methoxyiminomethylbenzoic acid, 2 l of toluene, 3 mL of dimethylformamide and 104 g (64 mL) of thionyl chloride. The resulting mixture was heated at 70° C. for 2 hours, filtered while hot and the solvent removed using a rotary evaporator yielding 178.1 g of the expected 4-amino-3-chloro-5-methoxyiminomethylbenzoyl chloride.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05874466 |
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| 출처 데이터셋 | uspto-grants-1999_02 |
|---|
| ORD ID | ord-093d5ecf5a8647b684fe6f3e10bff9f9 |
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| 출처 메모 | uspto-grants-1999_02 |
|---|
