Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Chlorotrimethylsilane → Silane, trimethyl[[2-methyl-1-(1-methylethyl)-1-propenyl]oxy]-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Chlorotrimethylsilane | HCID 6397 | — |
| 반응물 | 2,4-Dimethyl-3-pentanone | HCID 11271 | — |
| 생성물 | Silane, trimethyl[[2-methyl-1-(1-methylethyl)-1-propenyl]oxy]- | HCID 11095327 | — |
반응 단계
Reaction between 2,4-dimethyl-3-pentanone (1.2.4.3), trimethylsilyl chloride, and base gave 2,4-dimethyl-3-trimethysilyloxy-2-pentene (1.2.4.4) which was reacted with 1-fluoropyridinium triflate (1.2.4.5) to form 2,4-dimethyl-2-fluoro-3-pentanone (1.2.4.6). This product was reacted with (CH3)3S(O)+I- to form the title compound (1.2.4.2). ##STR31##
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05874573 |
| 출처 데이터셋 | uspto-grants-1999_02 |
| ORD ID | ord-12c500d629034589a9aeeb6f309ba54c |
| 출처 메모 | uspto-grants-1999_02 |