Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethyl Acetate → Benzenebutanal, 4-(phenylmethoxy)-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethyl Acetate | HCID 8857 | — |
| 반응물 | Sulfuric acid magnesium salt (1:1) | HCID 24083 | — |
| 반응물 | Norepinephrine | HCID 439260 | — |
| 촉매 | Platinum | HCID 23939 | — |
| 생성물 | Benzenebutanal, 4-(phenylmethoxy)- | HCID 11086308 | — |
반응 단계
A solution of 4-(4-benzyloxyphenyl)-butanal (52.4 g, 206 mmol) in 150 mL ethyl acetate (1.4M solution) was prepared and set aside. 10% platinum on carbon (3.40 g) was prewetted with ethyl acetate and transferred to the reactor. To this was added magnesium sulfate (60.0 g, 500 mmol), followed by the ethyl acetate solution of (trimethylsilyl)-protected norepinephrine prepared as described in Example 1.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05874601 |
| 출처 데이터셋 | uspto-grants-1999_02 |
| ORD ID | ord-becb9cf850d841398405eae6e1336a80 |
| 출처 메모 | uspto-grants-1999_02 |